Materials Characterisation

Thermogravimetric Analysis

tga_setaram2

Setaram Setsys CS Evolution

RT-1600 °C range, 30 °C/min maximum ramp

40g maximum weight, ±20 & ±200 mg ranges

Vacuum, air, N2, Ar, CO2, and dilute flammable gas environments

DSC capable

tga-TA_Q600

TA Instruments SDT Q600

Simultaneous TGA-DSC, dual cantilever beam type

RT-1500 °C range, 200 mg sample weight

25 °C/min maximum ramp (RT-1500°C)

100 °C/min maximum ramp (RT-1000°C)

Air, N2, Ar, CO2, and dilute flammable gas environments

Particle Size Analysis

psa2

Malvern Instruments Mastersizer 2000

Laser diffraction particle size analyzer

Red (633 nm) and blue (466 nm) laser light sources

Wet (Hydro 2000s) and dry (Scirocco 2000) dispersion units

Particle size limits: <600 µm (wet) & <2000 µm (dry)

 

sieveshaker

WS Tyler ROTAP Sieve Shaker

Uses 8" sieves

25, 32, 45, 75, 105 µm openings (others available)

Enclosed in ducted cabinet

ultrasonicshaker

Advantech SonicSifter L3P

Uses 3" acrylic sieves

5 & 10 µm openings (others available)

Horizontal tap accessory

 

Surface Area Analysis

AutoSorbiQ

Quantachrome Instruments Autosorb iQ

Gas sorption surface area and pore size analyzer for porous materials and powders

BET, HK, DA, BJH, & DR analysis methods

Mass spectrometry

mass_spec2

Hiden Analytical HPR20

Residual Gas Analyzer- quadrupole mass spectrometer

Microscopy

microscope_2

Zeiss Axio Scope A1 Optical Microscope

100x, 200x, & 400x magnification (reflected light microscopy)

AxioCam ICc1 digital camera

Dilatometry

dilatometer

Anter Unitherm 1161V

Thermal expansion/contraction measurements using vertical pushrods & LVDT

Vacuum, air, inert gas environments

RT-1650°C range

Zeta Potential

zetapotential

Matec Applied Sciences Zeta-APS

Simultaneous zeta potential, particle size distribution percent Solids, pH, conductivity, temperature, sound-attenuation and speed spectra.

Viscometer

viscometer_2

Thermo Scienctific Haake Viscotester 7 Plus